NMR Service

The net prices listed below refer to the measurement of pre-prepared samples ( i.e. weighted and dissolved in deuterated solvent of choice) delivered in NMR tubes (5 mm external diameter; at least “precision” quality). Solution level in the tube should not be lower than 4.5 cm (ca. 0.6 mL) and not higher than 5.5 cm (ca. 1 mL). Low-concentrated samples can be measured until requested signal to noise ratio is achieved. Time of the temperature experiments is counted from the beginning of the heating up to the end of cooling down of the sample. A properly filled request form should be attached to samples. Data files are available online on our servers. For any further details please contact us.

Request form I           

JEOL JNM-ECZL 400 MHz (HFX and Royal HFX probes)

Standard spectra:

1H NMR – 18.00 PLN;

19F NMR (without decoupling)  – 18.00 PLN

 31P NMR – 18.00 PLN

Other experiments:

80.00 PLN per hour of spectrometer work

AVANCE II PLUS 700 MHz (broadband BBO probe)

Standard spectra:

1H NMR – 23.00 PLN

 19F NMR (without decoupling) – 23.00 PLN

31P NMR – 23.00 PLN  

Other experiments:

100.00 PLN per hour of spectrometer work

Available solvents

  • Acetone-d6 (ampule;+ 12.00 PLN)
  • Acetonitrile-d3 (ampule;+ 15.00 PLN)
  • Benzene-d6 (+ 14.00 PLN)
  • Chloroform-d (+ 8.00 PLN)
  • Chloroform-d + TMS0.03% (v/v) (+ 8.00 PLN)
  • Chloroform-d (ampule; + 10.00 PLN)
  • Chloroform-d + TMS0.03% (v/v) (ampule; + 13.00 PLN)
  • Deuterium oxide (ampule;+ 5.00 PLN)
  • Dichloromethane-d2 (ampule;+ 45.00 PLN)
  • DMSO-d6 (ampule;+ 10.00 PLN)
  • DMF-d7 (ampule;+ 120.00 PLN)
  • MeOH-d4 (ampule;+ 27.00 PLN)
  • TFA-d1 (+ 10.00 PLN)
  • THF-d8 (ampule;+ 60.00 PLN)
  • Toluene-d8 (+ 22.00 PLN)
Contact

Lodz University of Technology
Faculty of Chemistry
Institute of Organic Chemistry

Żeromskiego 116, 90-924 Łódź

Tel.: (+42) 631-31-52 Ext. 21 (AVANCE DPX 250 MHz)

        (+42) 631-31-52 Ext. 23 (AVANCE II PLUS 700 MHz)

E-mail:

E-mail: